Experimental Organic Chemistry 3/e [Cranwell] 9781119952381

The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures.

The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills.

New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis.

頁數：686
版次：第3版
年份：2017年
規格：平裝/雙色
ISBN：9781119952381

PART 1: LABORATORY PRACTICE
1 Safety in the chemical laboratory
2 Glassware and equipment in the laboratory
3 Organic reactions: From starting materials to pure organic product
4 Qualitative analysis of organic compounds
5 Spectroscopic analysis of organic compounds
6 Keeping records: The laboratory notebook and chemical literature
PART 2: EXPERIMENTAL PROCEDURES
7 Functional group interconversions
8 Carbon–carbon bond-forming reactions
9 Experiments using enabling technologies
10 Projects
APPENDICES
Organic solvents
Spectroscopic correlation tables